Molecular Structure Analysis: Single-Crystal X-ray Diffraction
Single-crystal X-ray diffraction is a powerful method in chemistry and materials science that makes it possible to determine the three-dimensional structure of molecules in crystals. In a typical experiment, a monocrystalline specimen is irradiated using an X-ray source and the resulting diffraction pattern can be analyzed to determine structural parameters such as atomic positions, and interatomic distances and angles.
We offer diffraction measurements for a variety of crystalline samples and are particularly well equipped to measure diffraction patterns from weakly-diffracting crystals. More Information regarding our instrumentation and service below.
Other tools to consider: NMR Spectroscopy, Mass Spectrometry and CHNS Determination
Instruments
Rigaku Synergy-R (N25/1207)
X-ray Sources
- Cu Rotating Anode
Detection
- Hypix Arc 100°
Measurement Temperature Range
- 80 to 400 K
- Small Crystals, Needles
- Poorly diffracting Crystals
- Inorganic und metal-organic complexes
- Organic molecules (small to medium size)
Rigaku/Oxford SuperNova (N25/1207)
X-ray Sources
- Mo and Cu microfocus sealed X-ray tubes
Detection
- Atlas Charged-Coupled Device (CCD) Detector
- Active Area (circular): 135 mm diameter
Sample Temperature Range
- r.t. to -150 °C
- Inorganic und metal-organic complexes
- Organic molecules (small to medium size)
Contact Person
Lionel Kroner, M.Sc.
- +49 731 50-23183
- lionel.kroner(at)uni-ulm.de
Instrument Status
Synergy R: functioning normally
SuperNova: functioning normally
News and Updates
New Instrument Added:
Synergy-R Instrument with a modern HPC Detector und brillant Cu X-ray Source is now a part of CF EMMA.